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The aim from the lab was to complete an electrophilic fragrant substitution
of ferrocene. Acetic acid is applied in conjunction with phosphoric acid because
the catalyst to create monoacetylferrocene. The reagent and catalyst applied
deliver a lot less hazardous byproducts and therefore are considered a a great
deal safer greener approach to the Click to enter process which will
involve solid Lewis acids and acetylhalides. The item is 2 cyclopentene rings
joined by and iron atom in the idle and an acetyl team sure to a carbon on among
the cyclopentene rings. The reagents and products are proven underneath.
Process and backlink delivered by Professor Carol Higginbotham Central Oregon
Neighborhood College, Organic Chemistry II CH 242/335I. Position a heating stir
plate with a lab jack and fill a dish with h2o then put on top rated. Set a
stand driving the north face
borealis and fasten two clamps. Clamp a reflux condenser for the major clamp
and a 20ml round base flask to your lessen clamp.II. Weigh out 1.5g of ferrocene
and position it in to the flask as well as a magnetic stir bar. When the water
bathtub is sort of for the boiling position lower the spherical bottom flask
into the h2o bathtub and add five.0ml of acetic anhydride.
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